HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hexyn-1-ol → N-{[(Hex-5-yn-1-yl)oxy]carbonyl}-3-methyl-L-valine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hexyn-1-ol | HCID 70234 | — |
| Reactant | 3-Methyl-N-{[(pent-4-en-1-yl)oxy]carbonyl}-L-valine | HCID 45379928 | — |
| Product | N-{[(Hex-5-yn-1-yl)oxy]carbonyl}-3-methyl-L-valine | HCID 57431194 | — |
Reaction Steps
N-[(Hex-5-yn-1-yloxy)carbonyl]-3-methyl-L-valine was prepared according to the procedure for 3-methyl-N-[(pent-4-enyloxy)carbonyl]-L-valine by using hex-5-yn-1-ol instead of 4-pentenol. LRMS (ESI) m/z 256.2 [(M+H)+; calcd for C13H22NO4: 256.1].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08216999B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-64967fd888f64ace8590bc050b1862b2 |
| Source note | uspto-grants-2012_07 |