HCID 62074621, compound → HCID 62072580, compound

HRID 1512237Notes

Reaction equation

HRID 1512237 reaction equation
[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][C:9]2[N:16]=[CH:15][CH:14]=[CH:13][C:10]=2[C:11]#[N:12])=[CH:4][CH:3]=1>[Ni]>[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][C:9]2[C:10]([CH2:11][NH2:12])=[CH:13][CH:14]=[CH:15][N:16]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 62074621HCID 62074621, compound

Product 1

HCID 62072580HCID 62072580, compound

Reagents, catalysts & solvents 1

HCID 935NickelCatalyst

Procedure

The product of Example 62A and Raney/nickel were processed according to the method of Example 131C to provide the product. MS (ESI+) m/z 216 (M+H)+.

Workup

  1. customto provide the product

Sources & evidence

ORD record
ord-0554517ca5f84c2db3522be096fa2a39
Source dataset
uspto-grants-2012_07
Patent number
US08217067B2

Reaction notes

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