2,3-Dichlorophenyl Isothiocyanate → HCID 86082291, compound

HRID 1512307Notes

Reaction equation

HRID 1512307 reaction equation
Cl.[Br:2][C:3]1[CH:8]=[C:7]([CH2:9][NH2:10])[CH:6]=[CH:5][N:4]=1.[Cl:11][C:12]1[C:17]([Cl:18])=[CH:16][CH:15]=[CH:14][C:13]=1[N:19]=[C:20]=[S:21]>>[Br:2][C:3]1[CH:8]=[C:7]([CH2:9][NH:10][C:20]([NH:19][C:13]2[CH:14]=[CH:15][CH:16]=[C:17]([Cl:18])[C:12]=2[Cl:11])=[S:21])[CH:6]=[CH:5][N:4]=1

Participants

3

Reactant 2

HCID 27962812,3-Dichlorophenyl IsothiocyanateHCID 66569557(2-Bromopyridin-4-yl)methanamine hydrochloride

Product 1

HCID 86082291HCID 86082291, compoundYield 84%

Procedure

Prepared in 84% yield from the product of Example 144A and 2,3-dichlorophenylisothiocyanate according to the procedure described for Example 141B and 141C.

Sources & evidence

ORD record
ord-b42a51291337498ea2e9756145c1c7c0
Source dataset
uspto-grants-2012_07
Patent number
US08217067B2

Reaction notes

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