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2-Chlorophenyl chloroformate → 2-Chlorophenyl 4-(prop-2-ynyl)piperidine-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Chlorophenyl chloroformate | HCID 4184068 | — |
| 反応物 | Tert-butyl 4-(prop-2-yn-1-yl)piperidine-1-carboxylate | HCID 18187546 | — |
| 生成物 | 2-Chlorophenyl 4-(prop-2-ynyl)piperidine-1-carboxylate | HCID 57838891 | — |
反応手順
2-(chloro)phenyl chloroformate (5.00 g, 26.2 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (4.50 g, 20.2 mmol) according to general procedure 1. Yield=4.56 g, 82%. m/z MH+=278.13. HPLC rt=9.3 min.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08222228B2 |
| 出典データセット | uspto-grants-2012_07 |
| ORD ID | ord-6acc65df49854c04a7b526eac665adfe |
| 出典メモ | uspto-grants-2012_07 |