Cyclohexylamine → HCID 24825959, compound

HRID 1514352Notes

Reaction equation

HRID 1514352 reaction equation
Cl[C:2]1[N:7]=[C:6](Cl)[CH:5]=[C:4]([CH3:9])[N:3]=1.[CH:10]1([NH2:16])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1.[NH:17]1[C:25]2[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH:19]=[N:18]1>>[CH:10]1([NH:16][C:6]2[CH:5]=[C:4]([CH3:9])[N:3]=[C:2]([N:17]3[C:25]4[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=4)[CH:19]=[N:18]3)[N:7]=2)[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1

Participants

4

Reactant 3

HCID 7965CyclohexylamineHCID 92211H-IndazoleHCID 794712,4-Dichloro-6-methylpyrimidine

Product 1

HCID 24825959HCID 24825959, compound

Procedure

Was prepared according to Method A from 2,4-dichloro-6-methylpyrimidine, cyclohexylamine and indazole. LC-ESI-HRMS of [M+H]+ shows 308.1859 Da. Calc. 308.18752 Da, dev. −5.3 ppm.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-3869efdaa8a34f68b53466c775cb7300
Source dataset
uspto-grants-2012_07
Patent number
US08222262B2

Reaction notes

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