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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1514780Generated: October 25, 2026

(+)-Solketal → (2S)-2,3-Bis(nitrooxy)propan-1-ol

https://huagongshe.com/reaction/1514780

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(+)-SolketalHCID 736057—
Reactant(2S)-3-(2,2-Dimethyl-1,1-diphenyl-1-silapropoxy)propane-1,2-diolHCID 10806357—
Reactant(2R)-2,3-bis(nitroxy)propan-1-olHCID 73416231—
Product(2S)-2,3-Bis(nitrooxy)propan-1-olHCID 73416232—

Reaction Steps

The title compound was prepared in four steps from ((4S)-2,2-dimethyl-1,3-dioxolan-4-yl)methan-1-ol following the procedures for Examples 5a, 5b, 5c, and 5d.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08222277B2
Source datasetuspto-grants-2012_07
ORD IDord-e181eceba8a840329f356f9794ce3dda
Source noteuspto-grants-2012_07