HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1514829Generated: November 3, 2026
2,6-Di-tert-butyl-4-methylphenol → HCID 68545777, compound
https://huagongshe.com/reaction/1514829
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,6-Di-tert-butyl-4-methylphenol | HCID 31404 | — |
| Reactant | 2-Propenoic acid, 3-hydroxypropyl ester | HCID 33101 | — |
| Reactant | N,N',N''-Tris(3-dimethylaminopropyl)hexahydro-S-triazine | HCID 85160 | — |
| Reactant | Isocyanate | HCID 105034 | — |
| Reactant | 1-Isocyanato-2-(methylsulfanyl)benzene | HCID 2736989 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68545777 | HCID 68545777 | — |
Reaction Steps
0.008 g of 2,6-di-tert-butyl-4-methylphenol, 0.004 g of Desmorapid Z, 4.8 g of 2-(methylthio)phenyl isocyanate in 8.5 g of ethyl acetate were initially introduced into a 50 ml round-bottomed flask and heated to 60° C. Thereafter, 3.7 g of 3-hydroxypropyl acrylate were added dropwise and the mixture was kept further at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, the ethyl acetate was distilled off at 5 mbar and cooling was effected. The product was obtained as a light yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08222314B2 |
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| Source dataset | uspto-grants-2012_07 |
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| ORD ID | ord-417b1ef1ffb447e781f645e67c27775e |
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| Source note | uspto-grants-2012_07 |
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