Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Sorbic Acid | HCID 643460 | — |
| Catalyst | Tetraethylammonium Bromide | HCID 6285 | — |
| Solvent | Water | HCID 962 | — |
| Product | 63623-06-3 | HCID 6446708 | — |
Reaction Steps
To 1.8 g of sorbic acid (manufactured by Wako Pure Chemical) were added 1 g of tetraethylammonium bromide (manufactured by Wako Pure Chemical) and 60 ml of epichlorohydrin (manufactured by Wako Pure Chemical), the mixture was heated to reflux at 110° C. for 3 hours, 30 ml of distilled water was added thereto and an organic layer was separated and concentrated in vacuoat 80° C. to give 3.5 g of glycidyl sorbate. An epoxy equivalent of this glycidyl sorbate was 367.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08222399B2 |
|---|
| Source dataset | uspto-grants-2012_07 |
|---|
| ORD ID | ord-c02aa7a0436b426fb7784a06870f5a18 |
|---|
| Source note | uspto-grants-2012_07 |
|---|
