反应详情

The title compound was prepared from 3,4-diamino-N-quinolin-2-yl-benzamide and [(E)-3-(4-formyl-3,5-dimethylphenyl)-allyl]-phosphonic acid diethyl ester analogous to Example 6-32. 1H NMR (Methanol-d4, 400 MHz): δ 8.42 (m, 3H), 8.05 (dd, 1H), 7.94 (dd, 2H), 7.79 (dd, 1H), 7.77 (m, 1H), 7.56 (m, 1H), 7.09 (s, 2H), 2.75 (t, 2H), 2.18 (s, 6H), 2.00 (m, 2H), 1.69 (m, 2H). MS (m/z) 543.2 (M+1); Retention time: 1.13 min (Method 10).