Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isoluminol → HCID 59479520, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isoluminol | HCID 95014 | — |
| 반응물 | 3,4-Dimethoxyphenylboronic acid | HCID 2734702 | — |
| 반응물 | Glyoxylic acid, monohydrate | HCID 15620607 | — |
| 반응물 | 2-(3-Carbamoyl-4-fluorophenylamino)-2-(3,4-dimethoxyphenyl)acetic acid | HCID 59479392 | — |
| 생성물 | HCID 59479520 | HCID 59479520 | 95% |
반응 단계
15A was prepared in a procedure similar to that of 13A using 6-amino-2,3-dihydrophthalazine-1,4-dione, 3,4-dimethoxyphenylboronic acid and glyoxylic acid monohydrate. Yield: 95%. 1H NMR (400 MHz, DMSO-d6) δ ppm 3.73 (s, 3H) 3.74 (s, 3H) 5.15 (d, J=7.03 Hz, 1H) 6.95 (d, 1H) 7.01-7.06 (m, 1H) 7.13 (d, J=2.20 Hz, 1H) 7.25 (d, J=7.03 Hz, 2H) 7.74 (s, 1H), LCMS: 344 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08222453B2 |
| 출처 데이터셋 | uspto-grants-2012_07 |
| ORD ID | ord-c6bc909f9a9744d78b2a1d40ce22d8d5 |
| 출처 메모 | uspto-grants-2012_07 |