HRID1515522
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Example 33 was prepared according to the general coupling condition using 29A and 31A. 1H NMR (400 MHz, Methanol-d4) δ ppm 1.19 (d, J=6.59 Hz, 3 H) 1.31 (t, J=7.03 Hz, 3H) 1.44 (d, J=6.59 Hz, 3H) 1.68-1.81 (m, 1H) 1.99-2.09 (m, 1H) 2.08-2.19 (m, 1H) 2.40-2.57 (m, 1H) 3.00 (s, 6H) 3.69-3.78 (m, 1H) 3.79-3.89 (m, 1H) 3.90-4.02 (m, 2H) 4.11-4.20 (m, 1H) 5.44 (s, 1H) 5.65 (dd, J=8.35, 5.27 Hz, 1H) 6.80 (d, J=2.20 Hz, 1H) 6.96-7.05 (m, 4H) 7.10-7.19 (m, 1 H) 7.30 (d, J=8.79 Hz, 2H) 7.71 (d, J=8.35 Hz, 1H), LCMS: 672 (M+1).
WORKUP
后处理
- customExample 33 was prepared