HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 11561969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | [1,1′:3′,1′′-Terphenyl]-4-carboxylic acid, 4′′-(diethylamino)-3′′-(1,1-dimethylethyl)-4′-(3-hydroxypropyl)- | HCID 11525429 | — |
| Reactant | HCID 11641897 | HCID 11641897 | — |
| Product | HCID 11561969 | HCID 11561969 | 86% |
Reaction Steps
In a manner similar to that of Example 3, by reacting 70 mg of ethyl 3″-tert-butyl-4″-diethylamino-4′-(2,3-dihydroxypropyl)-[1,1′;3′,1″]terphenyl-4-carboxylate (0.14 mmol) with 0.2 mL of 1N sodium hydroxide solution, 58 mg of 3″-tert-butyl-4″-diethylamino-4′-(3-hydroxypropyl)-[1,1′;3′,1″]terphenyl-4-carboxylic acid are obtained (yield=86%) in the form of a white solid (m.p.=130° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08227507B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-6240a5e40c3643179e401b367bf52d08 |
| Source note | uspto-grants-2012_07 |