Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methylpyridine → 2-Acetoxy-4-methylpyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methylpyridine | HCID 7963 | — |
| 반응물 | Acetyl hypofluorite | HCID 127602 | — |
| 반응물 | HCID 178428601 | HCID 178428601 | — |
| 생성물 | 2-Acetoxy-4-methylpyridine | HCID 12258188 | — |
반응 단계
As a process for the preparation of 2-hydroxy-4-methylpyridine, a process whereby [iv] 4-methylpyridine is reacted with acetyl hypofluorite at −10° C. to obtain a 2-acetoxy-4-methylpyridine, and thereafter the 2-acetoxy-4-methylpyridine is hydrolyzed to obtain 4-methyl-2-pyridone is reported [Journal of the American Chemical Society, 109, 3789-3790, (1987): Non-Patent Reference 2].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08227617B2 |
| 출처 데이터셋 | uspto-grants-2012_07 |
| ORD ID | ord-134324e128ff46398b4c24f101b11fde |
| 출처 메모 | uspto-grants-2012_07 |