反应详情

温度

60 °C

To 400 ml of toluene are added 30 g of 1-(4-aminophenyl)propan-1-one and 38 ml (402 mM) of acetic anhydride. The reaction medium is heated at 60° C. with stirring for 1 hour. A solid precipitates out. After filtration and washing with toluene, 37.9 g of N-(4-propanoylphenyl)acetamide are obtained in the form of a white powder.

1. customA solid precipitates out
2. filtrationAfter filtration
3. washwashing with toluene, 37.9 g of N-(4-propanoylphenyl)acetamide
4. customare obtained in the form of a white powder