Dimethylamine → HCID 67167880, compound

HRID 1517570Notes

Reaction equation

HRID 1517570 reaction equation
[CH:1]([C:3]1[C:4]([N:9]2[CH:13]=[C:12]([C:14]([O:16][CH2:17][CH3:18])=[O:15])[C:11]([CH3:19])=[N:10]2)=[N:5][CH:6]=[CH:7][CH:8]=1)=O.[CH3:20][NH:21][CH3:22]>>[CH3:20][N:21]([CH2:1][C:3]1[C:4]([N:9]2[CH:13]=[C:12]([C:14]([O:16][CH2:17][CH3:18])=[O:15])[C:11]([CH3:19])=[N:10]2)=[N:5][CH:6]=[CH:7][CH:8]=1)[CH3:22]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 58268583HCID 58268583, compound

Product 1

HCID 67167880HCID 67167880, compoundYield 95%

Procedure

This compound is prepared essentially as described in Preparation 7 by using ethyl 1-(3-formyl-2-pyridyl)-3-methyl-pyrazole-4-carboxylate and dimethylamine in a 95% yield and is used with no further purification after workup. MS (m/z): 289 (M+1)

Workup

  1. customThis compound is prepared essentially
  2. customas described in Preparation 7
  3. customis used with no further purification after workup

Sources & evidence

ORD record
ord-96efd4a22f7941b999823ff93e38a987
Source dataset
uspto-grants-2012_07
Patent number
US08232289B2

Reaction notes

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