HRID1517576
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of [1-(3-fluoro-2-pyridyl)-3-(isopropoxymethyl)pyrazol-4-yl]methanol (241 mg; 0.91 mmol) and manganese(IV) oxide (791 mg) are stirred in dichloromethane (5 mL) at room temperature overnight. After that time, the reaction mixture is filtered over celite and solvent evaporated to obtain 197 mg of the title compound that is used without further purification. MS (m/z): 264 (M+1).
WORKUP
后处理
- filtrationAfter that time, the reaction mixture is filtered over celite and solvent
- customevaporated