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HRID1517821

反应详情

EQUATION

反应方程式

HRID 1517821 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：COc1ccc2c(Oc3ccc(NC(=O)c4c(C)n(C[C@H](C)OC(=O)[C@H](C)N)n(-c5ccccc5)c4=O)cc3F)ccnc2c1
HCID59491006

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(Oc3ccc(NC(=O)c4c(C)n(C[C@H](C)OC(=O)[C@H](C)N)n(-c5ccccc5)c4=O)cc3F)ccnc2c1.O=S(=O)(O)O
HCID66669832

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 13 Step 3 by using (2S)—(S)-1-(4-(4-(7-methoxyquinolin-4-yloxy)-3-fluorophenyl-carbamoyl)-2,3-dihydro-5-methyl-3-oxo-2-phenylpyrazol-1-yl)propan-2-yl 2-aminopropanoate (61.3 mg, 0.1 mmol) and H2SO4 (1 mL, 0.1 mol/L, Shantou Xilong Chemical Factory). The title compound was obtained as a yellow solid (61.5 mg, 86.5%).

WORKUP

后处理

  1. customThe title compound was prepared