HRID1517943
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
6.8 g tert-butyl 5-nitro-indole-1-carboxylate are dissolved in 120 ml of methanol. 600 mg palladium on charcoal (10%) are added thereto and the mixture is hydrogenated for 1.5 hours at ambient temperature. Then the catalyst is filtered off and the solvent is eliminated in vacuo.
WORKUP
后处理
- filtrationThen the catalyst is filtered off