Benzoyl chloride → HCID 178463785, compound

Participants

Reaction Steps

5-Amino-6-diethylamino-2-(cyclohexyl)-1H-benzo[d]-imidazole (27 mg, 0.1 mmol) was reacted with benzoyl chloride (11 mg, 0.1 mmol) in the same manner as that described above to give the desired product (27 mg, 74% yield) as white powder: 1H-NMR (300 MHz, CDCl3) δ 0.98 (t, 6H, J=7.2 Hz), 1.16 (m, 3H), 1.57-1.70 (m, 5H), 1.98 (m, 2H), 2.87 (m, 1H), 3.03 (q, 4H, J=7.2 Hz), 7.57 (m, 3H), 7.57 (s, 1H), 8.00 (dd, 2H, J=1.8, 8.4 Hz), 8.96 (s, 1H); ESI MS m/z 391.0 [M+H]+.

Provenance & Evidence