돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1518174생성일: 2026년 10월 25일

Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester → Hydroxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester

https://huagongshe.com/reaction/1518174

반응식

참여 물질

역할이름HCID투입량
반응물Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl esterHCID 57667396—
촉매PalladiumHCID 23938—
용매MethanolHCID 887—
생성물Hydroxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl esterHCID 57667367—

반응 단계

Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester 4 (5 grams) was dissolved in methanol (50 mL) in a pressure vessel, palladium on carbon (5%, 5 grams) was added and the mixture was stirred under an atmosphere of hydrogen (4 Kg) for 4 hours. The catalyst was removed by filtration and the methanol was distilled off to yield crude 5.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08232422B2
출처 데이터셋uspto-grants-2012_07
ORD IDord-3a5c37b98057400886749780a484c000
출처 메모uspto-grants-2012_07