HCID 46836570, compound → HCID 46836718, compound

Participants

Reaction Steps

The title compound 9 was prepared by following the procedure set forth in Example 6 but substituting compound 4 in Example 6 with compound 5: 1H NMR (300 MHz, DMSO-d6) δ ppm 12.89 (1H, s), 8.03 (1H, m), 7.79 (1H, d), 7.67 (1H, m), 7.42 (4H, m), 7.02 (1H, m), 6.33 (3H, m), 4.83 (2H, s), 3.90 (2H, t), 3.72 (2H, t), 3.16 (2H, m), 3.03 (2H, t), 1.98 (2H, m); MS (ESI(+)): m/z 586 (M+H).

Provenance & Evidence