Ethanol → HCID 86685007, compound

Participants

Reaction Conditions

Reaction Steps

N-phthaloyl protected 5-nonyloxy-4-azaindole (20 mg, 0.05 mmole) and hydrazine (3 mg, 0.09 mmole) was dissolved in CH2Cl2 (0.5 mL) in a 25 mL round bottom flask. EtOH (1 mL) was added to the reaction mixture and allowed to stir overnight at 25° C. for 12 h, after which it was cooled to 0° C., and filtered, and the white solid material was washed with 3 mL of cold CH2Cl2. The filtrate was evaporated under reduced pressure to afford 7 mg (50%) of 2-aminoethyl-5-nonyloxy-4-azaindole as a yellow solid. LRMS (ESI): M+1 for C18H29N3O calcd 304.4. found 304.4.

Provenance & Evidence