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2-(Quinolin-5-yl)acetic acid → Methyl 4-bromo-2-(2-(quinolin-5-yl)acetamido)thiophene-3-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Quinolin-5-yl)acetic acid | HCID 20533909 | — |
| 反応物 | Methyl 2-amino-4-bromothiophene-3-carboxylate | HCID 68754257 | — |
| 生成物 | Methyl 4-bromo-2-(2-(quinolin-5-yl)acetamido)thiophene-3-carboxylate | HCID 68754644 | — |
反応手順
Methyl 4-bromo-2-(2-(quinolin-5-yl)acetamido)thiophene-3-carboxylate was prepared from 2-(quinolin-5-yl)acetic acid (427 mg, 2.18 mmol) and methyl 2-amino-4-bromothiophene-3-carboxylate (514 mg, 2.18 mmol) according to protocol A. Retention time (min)=1.660, method [1], MS(ESI) 405.0 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09073891B2 |
| 出典データセット | uspto-grants-2015_07 |
| ORD ID | ord-c97e43cd7079462798d8f7f3a97f3aff |
| 出典メモ | uspto-grants-2015_07 |