HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-nitrothiophene → HCID 68755304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-nitrothiophene | HCID 220186 | — |
| Reactant | 4-Methyl-2-(tributylstannyl)-1,3-thiazole | HCID 16427130 | — |
| Product | HCID 68755304 | HCID 68755304 | — |
Reaction Steps
4-Methyl-2-(3-nitrothiophen-2-yl)thiazole was prepared from 2-chloro-3-nitrothiophene (219 mg, 1.34 mmol) and 4-methyl-2-(tributylstannyl)thiazole (520 mg, 1.34 mmol) according to protocol E. Retention time (min)=2.462, method [1], MS(ESI) 227.0 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073891B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-006aa5f909fa496a903b577d409445ef |
| Source note | uspto-grants-2015_07 |