HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-(2-Bromophenylsulfanyl)-2-chloro-4-methoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-Bromobenzenethiol | HCID 80598 | — |
| Reactant | 4-Amino-3-chlorophenol | HCID 87184 | — |
| Reactant | 2-Chloro-1-iodo-4-methoxybenzene | HCID 18001519 | — |
| Product | 1-(2-Bromophenylsulfanyl)-2-chloro-4-methoxybenzene | HCID 68682905 | — |
Reaction Steps
Prepared from 2-bromo-benzenethiol and 2-chloro-1-iodo-4-methoxy-benzene (prepared from 4-amino-3-chloro-phenol by diazotization according to the general procedure by Tunney and Stille J. Org. Chem. 1987, 52, 748-753 followed by alkylation with methyl iodide according to the general procedure by Uozumi et al. J. Org. Chem. 1993, 58, 1945-1945)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07732463B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-df4420fb03d3464ea084d114a4475e52 |
| Source note | uspto-grants-2010_06 |