HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → 1-Bromo-3-fluoro-2-(4-methoxy-phenylsulfanyl)-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | 2-Bromo-6-fluoroaniline | HCID 2782940 | — |
| Reactant | 1-Bromo-3-fluoro-2-iodobenzene | HCID 2783127 | — |
| Product | 1-Bromo-3-fluoro-2-(4-methoxy-phenylsulfanyl)-benzene | HCID 68682889 | — |
Reaction Steps
Prepared from 4-methoxy-benzenethiol and 1-bromo-3-fluoro-2-iodo-benzene (prepared from 2-bromo-6-fluoro-phenylamine by diazotization according to the general procedure by Tunney and Stille J. Org. Chem. 1987, 52, 748-753).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07732463B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-deecd597bab4449d99508d960324b959 |
| Source note | uspto-grants-2010_06 |