HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-4-morpholinobut-2-enoic acid → (E)-4-morpholino-N-(3-(4-(4-phenoxyphenoxy)pyridin-3-yl)phenyl)but-2-enamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-4-morpholinobut-2-enoic acid | HCID 22466617 | — |
| Reactant | 3-(4-(4-Phenoxyphenoxy)pyridin-3-yl)aniline | HCID 71474010 | — |
| Product | (E)-4-morpholino-N-(3-(4-(4-phenoxyphenoxy)pyridin-3-yl)phenyl)but-2-enamide | HCID 71092758 | 34% |
Reaction Steps
(E)-4-morpholino-N-(3-(4-(4-phenoxyphenoxy)pyridin-3-yl)phenyl)but-2-enamide was prepared from 3-(4-(4-phenoxyphenoxy)pyridin-3-yl)aniline and (E)-4-morpholinobut-2-enoic acid using Method E (34% yield). HPLC: 100%, RT=3.493 min. MS: m/z=508 [M+H]+, RT=2.27 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073947B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-07e1459a5d294a6ab35f1b50ce45c37f |
| Source note | uspto-grants-2015_07 |