HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 71092838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Reactant | HCID 71092760 | HCID 71092760 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71092838 | HCID 71092838 | 58% |
Reaction Steps
N-(3-(4-(4-phenoxyphenoxy)pyridin-3-yl)benzyl)propionamide was prepared from (3-(4-(4-phenoxyphenoxy)pyridin-3-yl)phenyl)methanamine and pyridine instead of N, N-diethylethanamine, 1-methylpyrrolidin-2-one, dichloromethane using Method G (58% yield). HPLC: 97%, RT=4.034 min. MS: m/z=425 [M+H]+, RT=3.34 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073947B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-f5ce330b40234d93821ddea55c4b813c |
| Source note | uspto-grants-2015_07 |