Acetic Acid → HCID 68478950, compound

Participants

Reaction Steps

A solution of 1-(2-Cyclohexyl-ethyl)-isatine (180 mg, 0.70 mmol) previously obtained (see isatine 2 in table 5) and Benzenesulfonyl hydrazide (120 mg, 0.70 mmol) in a solution of acetic acid, ethanol and THF (20%, 40%, 40%) is stirred at room temperature for 12 h. After concentration, a yellow precipitate is filtered and washed with ethanol to afford a desired product. M=239 mg, Yield: 83%.

Provenance & Evidence