HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-methylbutane → 1-Isopentyl-5-methylindoline-2,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-methylbutane | HCID 7891 | — |
| Reactant | 5-Methylisatin | HCID 11840 | — |
| Reactant | 1-propyl-1H-indole-2,3-dione | HCID 1645090 | — |
| Product | 1-Isopentyl-5-methylindoline-2,3-dione | HCID 4730242 | — |
Reaction Steps
Made in an analogous fashion to 1-propylindoline-2,3-dione using commercially available 5-methyl isatin (purchased from Fisher Scientific) and 1-bromo-3-methylbutane (purchased from Fisher Scientific). 1H NMR δ 7.41 (m, 2H), 6.78 (d, 1H), 3.71 (t, 2H), 2.33 (s, 3H), 1.57 (m, 3H), 0.99 (d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079853B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-d348c1ddb2744e24bdd4e236d40e3a9a |
| Source note | uspto-grants-2015_07 |