Methyl iodide → 3-Methoxy-2-methylpyridine

HRID 1523014Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6](C)=[N:7][CH:8]=1.O[C:11]1C(C)=NC=CC=1.CI>>[CH3:1][O:2][C:3]1[C:8]([CH3:11])=[N:7][CH:6]=[CH:5][CH:4]=1

Participants

Reactant 3

HCID 6328Methyl iodide

HCID 707192-Methylpyridin-3-ol

HCID 133587775-Methoxy-2-methylpyridine

Product 1

HCID 30152703-Methoxy-2-methylpyridine

Procedure

Was prepared in a similar manner to 5-methoxy-2-methylpyridine using 3-hydroxy-2-methylpyridine (purchased from Fisher Scientific) and methyl iodide (purchased from Fisher Scientific).

Sources & evidence

ORD record: ord-241f0c8ff9914722b782c1b32ebad20d
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09079853B2

Reaction notes

Loading…