化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Bromide → 1-ethyl-5-methyl-2,3-dihydro-1H-indole-2,3-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Bromide | HCID 6332 | — |
| 反応物 | 5-Methylisatin | HCID 11840 | — |
| 反応物 | 1-propyl-1H-indole-2,3-dione | HCID 1645090 | — |
| 生成物 | 1-ethyl-5-methyl-2,3-dihydro-1H-indole-2,3-dione | HCID 2471305 | — |
反応手順
Was prepared in an analogous manner to 1-propylindoline-2,3-dione using commercially available 5-methyl isatin (purchased from Fisher Scientific) and ethyl bromide (purchased from Fisher Scientific). 1H-NMR δ 7.42-7.38 (m, 2H), 6.80 (d, 1H), 3.77 (q, 2H), 2.34 (s, 3H), 1.31 (t, 3H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09079853B2 |
| 出典データセット | uspto-grants-2015_07 |
| ORD ID | ord-2d5057fbaff345b28e059dbdea3b6cdf |
| 出典メモ | uspto-grants-2015_07 |