HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatin → 1-butyl-1H-indole-2,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatin | HCID 7054 | — |
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | 1-propyl-1H-indole-2,3-dione | HCID 1645090 | — |
| Product | 1-butyl-1H-indole-2,3-dione | HCID 1581052 | — |
Reaction Steps
Was made in an analogous fashion to 1-propylindoline-2,3-dione by reacting commercially available isatin (purchased from Fisher Scientific) with 1-bromo-butane (purchased from Fisher Scientific). 1H-NMR δ 7.68 (m, 2H), 7.11 (dd, 1H), 6.90 (d, 1H), 3.72 (t, 2H), 1.65 (q, 2H), 1.41 (m, 2H), 0.97 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079853B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-5d37996d619849e2abab46deac6823b5 |
| Source note | uspto-grants-2015_07 |