HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → 5-Methyl-1-(4-methylpentyl)indoline-2,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | 5-Methylisatin | HCID 11840 | — |
| Reactant | 1-propyl-1H-indole-2,3-dione | HCID 1645090 | — |
| Product | 5-Methyl-1-(4-methylpentyl)indoline-2,3-dione | HCID 83157612 | — |
Reaction Steps
This compound was prepared in a similar method as 1-propylindoline-2,3-dione by reacting commercially available 5-methyl isatin (purchase from Fisher Scientific) with commercially available 1-bromo-5-methylpentane (purchase from Fisher Scientific). 1H NMR δ 7.42 (s, 1H), 7.38 (ddd, 1H), 6.79 (d, 1H), 3.68 (t, 2H), 3.34 (s, 3H), 1.69 (m, 2H), 1.60 (m, 1H), 1.27 (m, 2H), 0.88 (d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079853B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-8f1d497fc8734321bf3c2784c28d6761 |
| Source note | uspto-grants-2015_07 |