Diethyl Ether → HCID 89303250, compound

Participants

Reaction Steps

To a solution of compound (25) (1.35 g, 2.46 mmol) in absolute ethanol (100 ml) was added 10% Pd/C (0.41 g). The resultant mixture was stirred at an ambient temperature in the presence of H2 (g) for 12 hours. The reaction mixture was filtered through a celite pad and washed with ethanol (2×20 ml). The filtrate was evaporated in vacuo to give an oily residue, which was then treated with Et2O to obtain a white solid of compound (26) (1.25 g, 98% yield).

Provenance & Evidence