huagongshe.com
HRID1523948

反应详情

EQUATION

反应方程式

HRID 1523948 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)NS(=O)(=O)c1ccccc1Br
HCID4825014

2-bromo-N-tert-butylbenzenesulfonamide

C10H14BrNO2S

结构：CC1(C)OB(c2ccc(-c3nnc(N)s3)c(F)c2)OC1(C)C
HCID90314325

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)NS(=O)(=O)c1ccccc1-c1ccc(-c2nnc(N)s2)c(F)c1
HCID90313954

未命名化合物

PROCEDURE

实验过程

The title compound was prepared using analogous conditions to those described in Example 6 utilizing 5-(2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1,3,4-thiadiazol-2-amine and 2-bromo-N-(tert-butyl)benzenesulfonamide. MS (ESI): mass calcd. for C18H19FN4O2S2, 406.09; m/z found, 407.1 [M+H]+. 1H NMR (300 MHz, CD3OD) δ 8.20-8.10 (m, 2H), 7.69-7.56 (m, 2H), 7.46-7.36 (m, 3H), 1.08 (s, 9H).