HuagongsheHuagongshe Chemistry Print Report · For research reference only
2'-Bromoacetanilide → HCID 90313804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2'-Bromoacetanilide | HCID 136416 | — |
| Reactant | 5-(2-Fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl)-pyrazin-2-amine | HCID 90312276 | — |
| Product | HCID 90313804 | HCID 90313804 | — |
Reaction Steps
The title compound was prepared using analogous conditions to those described in Example 1 utilizing 5-(2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)pyrazin-2-amine and N-(2-bromophenyl)acetamide. MS (ESI): mass calcd. for C18H15FN4O, 322.12; m/z found, 322.9 [M+H]+. 1H NMR (400 MHz, DMSO-d6) δ 9.40 (s, 1H), 8.38 (s, 1H), 8.02 (s, 1H), 7.91 (m, 1H), 7.53-7.21 (m, 6H), 6.73 (s, 2H), 1.92 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079866B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-db6cf1b6f5174c66ad11caa4c987da9c |
| Source note | uspto-grants-2015_07 |