1-Bromo-2-fluorobenzene → HCID 90312837, compound

Participants

Reaction Steps

The title compound was prepared using analogous conditions to those described in Example 1 utilizing 5-(2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)pyrazin-2-amine and 2-bromofluorobenzene. MS (ESI): mass calcd. for C16H11F2N3, 283.09; m/z found, 284.1 [M+H]+. 1H NMR (600 MHz, CDCl3) δ 8.63-8.54 (m, 1H), 8.13 (d, J=1.4, 1H), 8.00 (m, 1H), 7.52-7.31 (m, 4H), 7.24-7.12 (m, 2H), 4.72 (s, 2H).

Provenance & Evidence