HCID 86708054, compound → HCID 86708055, compound

Participants

Reaction Steps

A solution of the material from Step 11 (110 mg, 0.126 mmol) in methanol (1 mL) was degassed with nitrogen, then 10% Pd/C (14 mg, 0.013 mmol) was added. The reaction mixture was stirred under hydrogen (1 atm) for 3 hours. The mixture was filtered through celite and washed with dichloromethane. The filtrate was concentrated in vacuo to afford 86 mg of the title compound which was used directly at Step 13. LCMS (M+1)=740

Provenance & Evidence