Benzamide → HCID 15173657, compound
Reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12])[C:5]([OH:7])=O.[C:15](N)(=O)C1C=CC=CC=1>>[Br:1][C:2]1[CH:3]=[C:4]([C:5](=[O:7])[CH3:15])[CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12]Participants
3
Procedure
3-Bromo-4,5-dimethoxybenzoic acid (2.0 g) was converted to the benzamide derivative analogously to O3.043, and the latter was converted to the title compound analogously to O2.059. 1.22 g of the title compound were obtained.
Sources & evidence
- ORD record
- ord-44347aabaf524d338fda0b31a6c2b82e
- Source dataset
- uspto-grants-2015_07
- Patent number
- US09079906B2
Reaction notes
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