HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4,5,6-trimethylpyrimidine → 2-Chloro-5-ethyl-4,6-dimethylpyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4,5,6-trimethylpyrimidine | HCID 12501987 | — |
| Reactant | HCID 178433497 | HCID 178433497 | — |
| Product | 2-Chloro-5-ethyl-4,6-dimethylpyrimidine | HCID 19846659 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Intermediate 56, substituting 5-ethyl-4,6-dimethylpyrimidin-2-ol for 4,5,6-trimethylpyrimidin-2-ol. MS (ESI): mass calculated for C8H11ClN2, 170.06, m/z found 171.1 [M+1]+. 1H NMR (500 MHz, CDCl3): 2.65 (q, J=7.6 Hz, 2H), 2.50 (s, 6H), 1.15 (t, J=7.6 Hz, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079911B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-9c00fc39fb06490a9426c26176d86c94 |
| Source note | uspto-grants-2015_07 |