3-Fluorobenzaldehyde → HCID 66576969, compound

HRID 1525405Notes

Reaction equation

[Cl:1][C:2]1[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[N:6][N:5]=[C:4]2[N:14]([CH3:24])[N:15]=[C:16]([C:17]3[CH:18]=[C:19](C)[CH:20]=[CH:21][CH:22]=3)[C:3]=12.[F:25]C1C=C(C=CC=1)C=O>>[Cl:1][C:2]1[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[N:6][N:5]=[C:4]2[N:14]([CH3:24])[N:15]=[C:16]([C:17]3[CH:22]=[CH:21][CH:20]=[C:19]([F:25])[CH:18]=3)[C:3]=12

Participants

Reactant 2

HCID 680093-Fluorobenzaldehyde

HCID 66576808HCID 66576808, compound

Product 1

HCID 66576969HCID 66576969, compound

Procedure

Compound 32 was synthesised following similar procedures outlined in Example 24 (Compound 19), using 3-fluorobenzaldehyde instead of 3-methylbenzaldehyde in Step 1.

Sources & evidence

ORD record: ord-b76530738e424e41b172efd8240021fe
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09079909B2

Reaction notes

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