Benzamide, 2-cyano- → HCID 131733154, compound

HRID 1525609Notes

Reaction equation

HRID 1525609 reaction equation
[C:1]([C:3]1[CH:11]=[CH:10][CH:9]=[CH:8][C:4]=1C(N)=[O:6])#N.[OH2:12].[OH2:13].O.O.O.O.[Co:18]([Cl:20])[Cl:19].O.O.O.O.O.O.[Co](Cl)[Cl:28].C(C1C=CC=CC=1C(N)=[O:35])#N>>[OH2:6].[OH2:35].[OH2:12].[OH2:6].[OH2:6].[OH2:6].[Co:18]([Cl:20])[Cl:19].[CH:10]1[CH:11]=[C:3]([C:1]([OH:13])=[O:12])[C:4]([Cl:28])=[CH:8][CH:9]=1

Participants

4

Reactant 3

HCID 72883Benzamide, 2-cyano-HCID 517166Dichlorocobalt hexahydrateHCID 131733155HCID 131733155, compound

Product 1

HCID 131733154HCID 131733154, compound

Procedure

To 5.13 g of 2-cyanobenzamide (2-CBA) (from Tokyo Chemical Industry Co., Ltd.) is added 1.39 g of cobalt (II) chloride hexahydrate (from Wako Pure Chemical Industries, Ltd.) and mixed in an agate mortar to prepare a cobalt (II) chloride hexahydrate/2-CBA mixture (18A).

Workup

  1. additionmixed in an agate mortar

Sources & evidence

ORD record
ord-6296dd9a17d846398bf9e4d729801109
Source dataset
uspto-grants-2015_07
Patent number
US09084992B2

Reaction notes

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