4-Methylpent-2-yne-1,4-diol → HCID 90389284, compound

HRID 1526594Notes

Reaction equation

HRID 1526594 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH3:12])[C:5]([C:8]([O:10][CH3:11])=[O:9])=[N:6][CH:7]=1.[CH3:13][C:14]([OH:20])([CH3:19])[C:15]#[C:16][CH2:17]O>>[OH:20][C:14]([CH3:19])([CH3:13])[C:15]#[C:16][CH2:17][O:1][C:2]1[CH:3]=[C:4]([CH3:12])[C:5]([C:8]([O:10][CH3:11])=[O:9])=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 827664-Methylpent-2-yne-1,4-diolHCID 90389409HCID 90389409, compound

Product 1

HCID 90389284HCID 90389284, compound

Procedure

The title compound was synthesized analogously according to Method S starting from methyl 5-hydroxy-3-methylpicolinate and 4-methylpent-2-yne-1,4-diol. MS m/z=264 (M+H)+.

Sources & evidence

ORD record
ord-853f85eb49bd4c1c8c282ec0c5ee4fc8
Source dataset
uspto-grants-2015_07
Patent number
US09085576B2

Reaction notes

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