Sodium Hydroxide → 2-(Ethylhydroxyphosphinyl)acetic acid sodium salt

HRID 1526930Notes

Reaction equation

[CH2:1]([P:3]([OH:9])([CH2:5][C:6]([OH:8])=[O:7])=[O:4])[CH3:2].[OH-].[Na+:11]>>[Na+:11].[CH2:1]([P:3]([OH:9])([CH2:5][C:6]([O-:8])=[O:7])=[O:4])[CH3:2]

Participants

Reactant 2

HCID 14798Sodium Hydroxide

HCID 15357685[Hydroxy(ethyl)phosphinyl]acetic acid

Product 1

HCID 462412532-(Ethylhydroxyphosphinyl)acetic acid sodium saltYield 98%

Procedure

An aqueous solution of 304 g (2 mol) of 2-(ethylhydroxyphosphinyl)acetic acid (prepared as in Example 9) is reacted with about 160 g of a 50% aqueous solution of sodium hydroxide and the water is distilled off in vacuo to leave 384 g (98% of theory) of 2-(ethylhydroxyphosphinyl)acetic acid sodium salt as colorless solid.

Workup

distillationthe water is distilled off in vacuo

Sources & evidence

ORD record: ord-a30522de1efd48cebf41e61a0e6cb1b1
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09085734B2

Reaction notes

Loading…