HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
methyl 2-(5-methoxy-1H-indol-3-yl)acetate → (1-Carbamoyl-5-methoxy-1H-indol-3-yl)-acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | methyl 2-(5-methoxy-1H-indol-3-yl)acetate | HCID 594955 | — |
| Edukt | (1-Carbamoyl-1H-indol-3-yl)-acetic acid | HCID 68283440 | — |
| Produkt | (1-Carbamoyl-5-methoxy-1H-indol-3-yl)-acetic acid | HCID 68284249 | — |
Reaktionsschritte
was prepared from 5-methoxy-3-indolylacetic acid methyl ester according to the protocol described scheme A8 for the preparation of (1-carbamoyl-1H-indol-3-yl)-acetic acid. Rf, TLC (EtOAC)=0.2; MS (LC/MS): 248.9 [M+H]+, 271.0 [M+Na]+, 247.1 [M−H]−, 495.1 [2M−H]−, 204.1 [M−CONH2]−; tR (HPLC conditions f): 1.54 min.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09085555B2 |
| Quelldatensatz | uspto-grants-2015_07 |
| ORD ID | ord-a20b10136a7e4a17973722a0388f08a9 |
| Quellennotiz | uspto-grants-2015_07 |