HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloroindole → (3-Acetyl-6-chloro-indol-1-yl)-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloroindole | HCID 87111 | — |
| Reactant | (3-Acetyl-5-trifluoromethoxy-indol-1-yl)acetic acid | HCID 68284505 | — |
| Product | (3-Acetyl-6-chloro-indol-1-yl)-acetic acid | HCID 68284278 | — |
Reaction Steps
was prepared from 6-chloro-1H-indole in a similar manner as described in Scheme A13 for the preparation of (3-acetyl-5-trifluoromethoxy-indol-1-yl)-acetic acid. Brown solid. MS: 252 [M+H]+, 274 [M+Na]+; tR (HPLC conditions k): 2.89 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09085555B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-8e140a34499549638e1a75b75c1a4514 |
| Source note | uspto-grants-2015_07 |