2-Bromo-3-methylpyridine → HCID 86673869, compound

HRID 1527527Notes

Reaction equation

HRID 1527527 reaction equation
Cl[C:2]1[C:3]([C:8]2[C:9]([F:15])=[C:10]([NH2:14])[CH:11]=[CH:12][CH:13]=2)=[N:4][CH:5]=[CH:6][CH:7]=1.Br[C:17]1C(C)=CC=CN=1>>[F:15][C:9]1[C:8]([C:3]2[C:2]([CH3:17])=[CH:7][CH:6]=[CH:5][N:4]=2)=[CH:13][CH:12]=[CH:11][C:10]=1[NH2:14]

Participants

3

Reactant 2

HCID 2208322-Bromo-3-methylpyridineHCID 68283569HCID 68283569, compound

Product 1

HCID 86673869HCID 86673869, compound

Procedure

was prepared by using the same procedures as described for the preparation of 3-(3-chloro-pyridin-2-yl)-2-fluoro-phenylamine in Scheme C6, starting from 2-bromo-3-methylpyridine [3430-17-9]. MS (LC-MS): 203 [M+H]+; tR (HPLC conditions k): 1.36 min.

Workup

  1. customwas prepared
  2. custom1.36 min.

Sources & evidence

ORD record
ord-0da9bf1320744483a6acc7bcb4b4947b
Source dataset
uspto-grants-2015_07
Patent number
US09085555B2

Reaction notes

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