2,3,4,5-Tetramethoxy-6-methylbenzaldehyde → HCID 46180173, compound

HRID 1527658Notes

Reaction equation

HRID 1527658 reaction equation
[CH3:1][C:2]1[C:7]([CH:8]=O)=[C:6]([O:10][CH3:11])[C:5]([O:12][CH3:13])=[C:4]([O:14][CH3:15])[C:3]=1[O:16][CH3:17].CC1C(/[CH:25]=[CH:26]/[C:27]([O:29][CH2:30][CH3:31])=[O:28])=C(OC)C(OC)=C(OC)C=1OC>>[CH3:1][C:2]1[C:7](/[CH:8]=[C:26](\[CH3:25])/[C:27]([O:29][CH2:30][CH3:31])=[O:28])=[C:6]([O:10][CH3:11])[C:5]([O:12][CH3:13])=[C:4]([O:14][CH3:15])[C:3]=1[O:16][CH3:17]

Participants

3

Reactant 2

HCID 148523342,3,4,5-Tetramethoxy-6-methylbenzaldehydeHCID 46180172HCID 46180172, compound

Product 1

HCID 46180173HCID 46180173, compound

Procedure

Compound 8b was prepared from 7 (0.569 g, 2.37 mmol) as described above for 8a to give 0.674 g (2.08 mmol, 88%) of the product as a yellow oil following flash chromatography (1:3 EtOAc:hexanes).

Sources & evidence

ORD record
ord-c3608446891b48178479e61ec8127282
Source dataset
uspto-grants-2015_07
Patent number
US09089605B2

Reaction notes

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