HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-3-(1,4-dimethoxynaphthalen-2-yl)-2-methylpropenoic acid → (E)-3-(1,4-dimethoxy-3-methylnaphthalen-2-yl)-2-nonylpropenoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-3-(1,4-dimethoxynaphthalen-2-yl)-2-methylpropenoic acid | HCID 46180242 | — |
| Reactant | Ethyl (E)-3-(1,4-dimethoxy-3-methylnaphthalen-2-yl)-2-nonylpropenoate | HCID 86647736 | — |
| Product | (E)-3-(1,4-dimethoxy-3-methylnaphthalen-2-yl)-2-nonylpropenoic acid | HCID 68741361 | — |
Reaction Steps
Compound 99c was prepared from 98c (0.164 g, 0.384 mmol) as described above for 29a to give 0.152 g (0.381 mmol, 96%) of the product as a colorless oil following flash chromatography (1:3 EtOAc:hexanes 0.5% AcOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09089605B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-c9d5f41aaf944d8a91b8beb7d84b03ec |
| Source note | uspto-grants-2015_07 |